Ammonia → HCID 11741307, compound

HRID 1611690Notes

Reaction equation

HRID 1611690 reaction equation
[CH2:1]([N:3]([CH2:11][CH3:12])[C:4]1[CH:5]=[C:6]([OH:10])[CH:7]=[CH:8][CH:9]=1)[CH3:2].[OH:13][C:14]1[CH:15]=[C:16]([CH:21]=[CH:22][CH:23]=1)[C:17](OC)=O.[NH3:24]>>[CH2:11]([N:3]([CH2:1][CH3:2])[C:4]1[CH:5]=[C:6]([CH:7]=[CH:8][CH:9]=1)[O:10][CH2:8][CH2:9][CH2:4][CH:5]([CH3:6])[O:13][C:14]1[CH:23]=[CH:22][CH:21]=[C:16]2[C:15]=1[N:24]=[C:1]([NH2:3])[CH:2]=[CH:17]2)[CH3:12]

Participants

4

Reactant 3

HCID 222AmmoniaHCID 70623-(Diethylamino)phenolHCID 88068Methyl 3-Hydroxybenzoate

Product 1

HCID 11741307HCID 11741307, compound

Procedure

The title compound was prepared according to the procedure described in Example 92 substituting 3-(diethylamino)phenol for methyl 3-hydroxybenzoate. 1H NMR (500 MHz, CDCl3) δ ppm 7.97 (d, 1H), 7.32 (t, 1H), 7.28 (m, 1H), 7.21 (dd, 1H), 7.15 (d, 1H), 7.06 (d, 1H), 6.90 (m, 2H), 6.74 (m, 1H), 4.69 (m, 1H), 4.11 (m, 1H), 4.05 (m, 1H), 3.49 (m, 4H), 2.21 (m, 1H), 2.08 (m, 1H), 1.93 (m, 2H), 1.46 (d, 3H), 1.11 (t, 6H); MS (DCI/NH3) m/z 394 [M+H]+.

Sources & evidence

ORD record
ord-edb7f7702f024760b74b2205804d9522
Source dataset
uspto-grants-2006_01
Patent number
US06989392B2

Reaction notes

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