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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1611690Generated: November 1, 2026

Ammonia → HCID 11741307, compound

https://huagongshe.com/reaction/1611690

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
Reactant3-(Diethylamino)phenolHCID 7062—
ReactantMethyl 3-HydroxybenzoateHCID 88068—
ProductHCID 11741307HCID 11741307—

Reaction Steps

The title compound was prepared according to the procedure described in Example 92 substituting 3-(diethylamino)phenol for methyl 3-hydroxybenzoate. 1H NMR (500 MHz, CDCl3) δ ppm 7.97 (d, 1H), 7.32 (t, 1H), 7.28 (m, 1H), 7.21 (dd, 1H), 7.15 (d, 1H), 7.06 (d, 1H), 6.90 (m, 2H), 6.74 (m, 1H), 4.69 (m, 1H), 4.11 (m, 1H), 4.05 (m, 1H), 3.49 (m, 4H), 2.21 (m, 1H), 2.08 (m, 1H), 1.93 (m, 2H), 1.46 (d, 3H), 1.11 (t, 6H); MS (DCI/NH3) m/z 394 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06989392B2
Source datasetuspto-grants-2006_01
ORD IDord-edb7f7702f024760b74b2205804d9522
Source noteuspto-grants-2006_01