HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 11741307, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 3-(Diethylamino)phenol | HCID 7062 | — |
| Reactant | Methyl 3-Hydroxybenzoate | HCID 88068 | — |
| Product | HCID 11741307 | HCID 11741307 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 92 substituting 3-(diethylamino)phenol for methyl 3-hydroxybenzoate. 1H NMR (500 MHz, CDCl3) δ ppm 7.97 (d, 1H), 7.32 (t, 1H), 7.28 (m, 1H), 7.21 (dd, 1H), 7.15 (d, 1H), 7.06 (d, 1H), 6.90 (m, 2H), 6.74 (m, 1H), 4.69 (m, 1H), 4.11 (m, 1H), 4.05 (m, 1H), 3.49 (m, 4H), 2.21 (m, 1H), 2.08 (m, 1H), 1.93 (m, 2H), 1.46 (d, 3H), 1.11 (t, 6H); MS (DCI/NH3) m/z 394 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06989392B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-edb7f7702f024760b74b2205804d9522 |
| Source note | uspto-grants-2006_01 |