HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 10068862, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 1-(p-Hydroxyphenyl)imidazole | HCID 82315 | — |
| Reactant | Methyl 3-Hydroxybenzoate | HCID 88068 | — |
| Product | HCID 10068862 | HCID 10068862 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 92 substituting 4-(1H-imidazol-1-yl)phenol for methyl 3-hydroxybenzoate. 1H NMR (500 MHz, CDCl3) δ ppm 8.89 (s, 1H), 7.93 (d, 1H), 7.45 (s, 1H), 7.38 (s, 1H), 7.32 (m, 3H), 7.20 (dd, 1H), 7.12 (d, 1H), 7.06 (d, 1H), 6.96 (m, 2H), 4.69 (m, 1H), 4.21 (m, 1H), 4.10 (m, 1H), 2.23 (m, 1H), 2.12 (m, 1H), 1.94 (m, 2H), 1.48 (d, 3H); MS (DCI/NH3) m/z 389 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06989392B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-f1ed3c50990f42438b796debcf188ce3 |
| Source note | uspto-grants-2006_01 |