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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1611695Generated: November 4, 2026

Ammonia → HCID 22254601, compound

https://huagongshe.com/reaction/1611695

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
Reactant3-CyanophenolHCID 13394—
ReactantMethyl 3-HydroxybenzoateHCID 88068—
ProductHCID 22254601HCID 22254601—

Reaction Steps

The title compound was prepared according to the procedure described in Example 92 substituting 3-cyanophenol for methyl 3-hydroxybenzoate. 1H NMR (500 MHz, DMSO-d6) δ ppm 8.36 (d, 1H), 7.47 (m, 2H), 7.42 (m, 2H), 7.35 (m, 1H), 7.31 (m, 1H), 7.20 (m, 1H), 7.12 (d, 1H), 4.87 (m, 1H), 4.10 (m, 2H), 1.78–2.07 (m, 4H), 1.40 (d, 3H); MS (DCI/NH3) m/z 348 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06989392B2
Source datasetuspto-grants-2006_01
ORD IDord-6b1e64f8b3024d9885664ab78d59612e
Source noteuspto-grants-2006_01