HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 22254601, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 3-Cyanophenol | HCID 13394 | — |
| Reactant | Methyl 3-Hydroxybenzoate | HCID 88068 | — |
| Product | HCID 22254601 | HCID 22254601 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 92 substituting 3-cyanophenol for methyl 3-hydroxybenzoate. 1H NMR (500 MHz, DMSO-d6) δ ppm 8.36 (d, 1H), 7.47 (m, 2H), 7.42 (m, 2H), 7.35 (m, 1H), 7.31 (m, 1H), 7.20 (m, 1H), 7.12 (d, 1H), 4.87 (m, 1H), 4.10 (m, 2H), 1.78–2.07 (m, 4H), 1.40 (d, 3H); MS (DCI/NH3) m/z 348 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06989392B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-6b1e64f8b3024d9885664ab78d59612e |
| Source note | uspto-grants-2006_01 |