HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 22254637, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 4-Cyanophenol | HCID 13019 | — |
| Reactant | Methyl 3-Hydroxybenzoate | HCID 88068 | — |
| Product | HCID 22254637 | HCID 22254637 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 92 substituting 4-cyanophenol for methyl 3-hydroxybenzoate. 1H NMR (500 MHz, DMSO-d6) δ ppm 8.36 (d, 1H), 7.70 (m, 2H), 7.44 (m, 3H), 7.12 (d, 1H), 7.00 (m, 2H), 4.84 (m, 1H), 4.12 (m, 2H), 1.74–2.05 (m, 4H), 1.40 (d, 3H); MS (DCI/NH3) m/z 348 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06989392B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-a7dc8867d625477ca06fed2daef4e3f7 |
| Source note | uspto-grants-2006_01 |