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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1611696Generated: November 1, 2026

Ammonia → HCID 22254637, compound

https://huagongshe.com/reaction/1611696

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
Reactant4-CyanophenolHCID 13019—
ReactantMethyl 3-HydroxybenzoateHCID 88068—
ProductHCID 22254637HCID 22254637—

Reaction Steps

The title compound was prepared according to the procedure described in Example 92 substituting 4-cyanophenol for methyl 3-hydroxybenzoate. 1H NMR (500 MHz, DMSO-d6) δ ppm 8.36 (d, 1H), 7.70 (m, 2H), 7.44 (m, 3H), 7.12 (d, 1H), 7.00 (m, 2H), 4.84 (m, 1H), 4.12 (m, 2H), 1.74–2.05 (m, 4H), 1.40 (d, 3H); MS (DCI/NH3) m/z 348 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06989392B2
Source datasetuspto-grants-2006_01
ORD IDord-a7dc8867d625477ca06fed2daef4e3f7
Source noteuspto-grants-2006_01