Cyanoacetamide → HCID 178509839, compound

HRID 1611736Notes

Reaction equation

HRID 1611736 reaction equation
[C:1](CC(N)=O)#[N:2].[OH:7][C:8]1[C:12]([C:13]#[N:14])=[C:11]([NH:15][C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[S:10][N:9]=1>>[OH:7][C:8]1[C:12]([C:13]#[N:14])=[C:11]([NH:15][C:16]2[CH:17]=[CH:18][CH:19]=[C:20]([C:1]#[N:2])[CH:21]=2)[S:10][N:9]=1

Participants

3

Reactant 2

HCID 7898CyanoacetamideHCID 178510528HCID 178510528, compound

Product 1

HCID 178509839HCID 178509839, compound

Procedure

The title compound was prepared from 1-isothiacyanato-3-cyano-benzene and 2-cyanoacetamide by the procedure analogous to Method 2 for 3-Hydroxy-5-phenylamino-isothiazol-4-carbonitrile. 1H NMR (CD3OD) δ: 7.5–7.7 (m, 4H) ppm; MS (ES, m/z): 242.9, [M-H]+, 241.1 [M-H]−.

Sources & evidence

ORD record
ord-a4e05381d3e4404b89d0cc5266d70a11
Source dataset
uspto-grants-2006_01
Patent number
US06989451B2

Reaction notes

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