HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 11289513, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ethyl 4-bromobutyrate | HCID 76300 | — |
| Reactant | 2,3,4-Trimethoxyphenol | HCID 603577 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 11289513 | HCID 11289513 | — |
Reaction Steps
9.2 g of trimethoxyphenol, 14 g of potassium carbonate and 10.7 g of ethyl 4-bromobutanoate in 150 ml of 2-butanone are refluxed for 24 hours. The mineral salts are then filtered off and the solvent is distilled off under reduced pressure, enabling the expected compound to be obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06992085B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-029f660a4bf0481fa87428c8836f6e6b |
| Source note | uspto-grants-2006_01 |