HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 22252351, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 22252333 | HCID 22252333 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22252351 | HCID 22252351 | — |
Reaction Steps
1 g of LiAlH4 is added in portions to a solution of 3 g of the compound obtained in Step A, in 100 ml of tetrahydrofuran, and then the reaction mixture is stirred for 8 hours, subsequently hydrolysed, filtered and finally evaporated to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06992085B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-db11236c17054f20b48eda3afa28bac8 |
| Source note | uspto-grants-2006_01 |