HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 17934199, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 22252720 | HCID 22252720 | — |
| Solvent | Tetrahydrofuran ethanol | HCID 21873804 | — |
| Product | HCID 17934199 | HCID 17934199 | — |
Reaction Steps
In a manner similar to that of Example 2, by reaction of 400 mg (0.92 mmol) of ethyl 6-(3-hydroxy-5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthylselanyl)nicotinate with 357 mg (8.9 mmol) of sodium hydroxide in a THF/ethanol mixture (20 ml/20 ml), 60 mg (16%) of a yellow powder are obtained. m.p.: 250° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06992094B1 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-d872d90c2f3d4178922d042e48e31ebe |
| Source note | uspto-grants-2006_01 |