HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 22252715, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Acetoxy-2-bromoethane | HCID 13564 | — |
| Reactant | HCID 22252718 | HCID 22252718 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 22252715 | HCID 22252715 | — |
Reaction Steps
In a manner similar to that of Example 51, by reaction of 400 mg (0.93 mmol) of ethyl 4-(3-hydroxy-5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthylselanyl)benzoate with 334 mg (2.2 mmol) of 2-bromoethyl acetate and 257 mg of potassium carbonate in MEK (10 ml), 333 mg (69%) of a yellow oil are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06992094B1 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-1555ba334be94ed596a8ce2ad50c723d |
| Source note | uspto-grants-2006_01 |