HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 86602661, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 9844045 | HCID 9844045 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86602661 | HCID 86602661 | — |
Reaction Steps
2 g (5 mmol) of 6-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthylselanyl)nicotinic acid, 20 ml of toluene, 100 μl of DMF and 450 μl of thionyl chloride are introduced into a round-bottomed flask. The reaction medium is refluxed for one hour and evaporated. 100% of the expected acid chloride are collected, this product being used for the rest of the synthesis without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06992094B1 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-efe05f2fd0f84056abb5b2be851fed61 |
| Source note | uspto-grants-2006_01 |