HRID1612068

反应详情

EQUATION

反应方程式

HRID 1612068 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Compound 13B (92 mg, 0.398 mmol) and 10% Pd/C (10 mg) in MeOH (5 mL) was hydrogenated under a hydrogen balloon for 30 minutes. The mixture was filtered and the filtrate concentrated under reduced pressure to give the title compound (80 mg).

WORKUP

后处理

  1. customfor 30 minutes
  2. filtrationThe mixture was filtered
  3. concentrationthe filtrate concentrated under reduced pressure