HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-nitro-1-naphthoate → Methyl 4-aminonaphthalene-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-nitro-1-naphthoate | HCID 825925 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 4-aminonaphthalene-1-carboxylate | HCID 10821944 | 99.9% |
Reaction Steps
Compound 13B (92 mg, 0.398 mmol) and 10% Pd/C (10 mg) in MeOH (5 mL) was hydrogenated under a hydrogen balloon for 30 minutes. The mixture was filtered and the filtrate concentrated under reduced pressure to give the title compound (80 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06992102B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-9eb753782d6e4021b4470525957aef22 |
| Source note | uspto-grants-2006_01 |