HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methoxyindan-1-one oxime → 5-methoxy-2,3-dihydro-1H-inden-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methoxyindan-1-one oxime | HCID 288189 | — |
| Reactant | 6,7-Dihydro-5H-cyclopenta[b]pyridin-5-amine | HCID 22147391 | — |
| Product | 5-methoxy-2,3-dihydro-1H-inden-1-amine | HCID 3016740 | — |
Reaction Steps
Following the procedure for the preparation of 6,7-dihydro-5H-cyclopenta[b]pyridin-5-amine but substituting 5-methoxyindan-1-one oxime and making non-critical variations provided the title compound as a oil: 1H NMR (CDCl3) δ 1.73, 2.75, 2.80, 2.94, 3.82, 4.34, 6.80, 7.25; HRMS (FAB) calcd for C10H11NO+H 162.0919, found 162.0922.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06992087B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-ff5eae21f77a43fbbedf54cb07cda22a |
| Source note | uspto-grants-2006_01 |