HCID 69587003, compound → HCID 23594222, compound

Participants

Reaction Steps

Compound 9c was prepared by following the procedure of Example 7, Step h, except 8c was substituted for 8a. (87%) 1H NMR (400 MHz, CDCl3) δ 7.07-7.36 (m, 9H), 6.11 (m, 1H), 5.80 (m, 1H), 4.39 (m, 2H), 3.76 (m, 2H), 2.78-3.19 (m, 2H), 2.71 (s, 4H), 2.49 (m, 2H), 2.01 (m, 3H), 1.75 (m, 5H). Mass Spectral Analysis m/z=394.3. (M+H)+ tR=3.13 min (99%)

Provenance & Evidence