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HRID1612477

反应详情

EQUATION

反应方程式

HRID 1612477 的结构方程式

REACTANTS

反应物

1
结构：C=CCOc1cc(C(=O)N[C@@H](Cc2ccccc2)[C@@H](O)C[C@@H](C)C(=O)NCCC(C)(C)C)cc(N2CCCC2=O)c1
HCID10196598

未命名化合物

PRODUCTS

生成物

1
结构：CCCOc1cc(C(=O)N[C@@H](Cc2ccccc2)[C@@H](O)C[C@@H](C)C(=O)NCCC(C)(C)C)cc(N2CCCC2=O)c1
HCID10175116

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：O=S(=O)([O-])[O-].O=S(=O)([O-])[O-].[Ba+2].[Pd+2]
催化剂HCID17887766

未命名化合物

结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

The allyl compound of E3 (0.042 g) was hydrogenated in methanol (5 ml) in the presence of 5% palladium-barium sulfate (0.020 g) for 3 hrs. The mixture was filtered through celite and evaporated to give the title compound.

WORKUP

后处理

  1. filtrationThe mixture was filtered through celite
  2. customevaporated