HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acrylate → Ethyl 3-{N-[3-(pyrid-4-yl)propyl]-N-methyl-amino}-propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | N-Methyl-3-(pyridin-4-yl)propan-1-amine | HCID 21974070 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Ethyl 3-{N-[3-(pyrid-4-yl)propyl]-N-methyl-amino}-propionate | HCID 19776451 | — |
Reaction Steps
15.1 g of ethyl acrylate are added portionwise to a solution of 22.5 g (0,15 Mol) of N-[3-(pyrid-4-yl)propyl]-N-methyl-amine in 50 ml of diethyl ether. The clear solution formed is allowed to stand overnight. The solvent is evaporated off. Ethyl 3-{N-[3-(pyrid-4-yl)propyl]-N-methyl-amino}-propionate is thus obtained as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05190930 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-9d18e73defdc4860a3325a50d2b43f80 |
| Source note | uspto-grants-1993_03 |