Hydrochloric Acid → HCID 19776538, compound

Participants

Reaction Steps

Dry HCl gas is introduced at 0°-10° C. over a period of half an hour into a solution of 0.5 g (2.732 mmol) of 2-(5-pyrimidylimino)-1,3-dithietane in 50 ml of diethyl ether. The resulting product is filtered off, washed with diethyl ether and dried, yielding 0.5 g (83.4% of the theoretical yield) of product having a melting point (decomp.) of 150° C. and above.

Provenance & Evidence