Hydrochloric Acid → HCID 19776538, compound

HRID 1612654Notes

Reaction equation

HRID 1612654 reaction equation
[ClH:1].[N:2]1[CH:7]=[C:6]([N:8]=[C:9]2[S:12][CH2:11][S:10]2)[CH:5]=[N:4][CH:3]=1>C(OCC)C>[ClH:1].[N:4]1[CH:5]=[C:6]([N:8]=[C:9]2[S:10][CH2:11][S:12]2)[CH:7]=[N:2][CH:3]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 19776539HCID 19776539, compound

Product 1

HCID 19776538HCID 19776538, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

Dry HCl gas is introduced at 0°-10° C. over a period of half an hour into a solution of 0.5 g (2.732 mmol) of 2-(5-pyrimidylimino)-1,3-dithietane in 50 ml of diethyl ether. The resulting product is filtered off, washed with diethyl ether and dried, yielding 0.5 g (83.4% of the theoretical yield) of product having a melting point (decomp.) of 150° C. and above.

Workup

  1. filtrationThe resulting product is filtered off
  2. washwashed with diethyl ether
  3. customdried
  4. customyielding 0.5 g (83.4% of the
  5. customtheoretical yield) of product
  6. customa melting point (decomp.) of 150° C.

Sources & evidence

ORD record
ord-bcb9480113314675be39778160ceeb8e
Source dataset
uspto-grants-1993_03
Patent number
US05190945

Reaction notes

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