HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumaric Acid → HCID 19776795, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | HCID 19776730 | HCID 19776730 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19776795 | HCID 19776795 | 79.6% |
Reaction Steps
Into 40 ml of ethanol were dissolved at first 1.0 g of 4-diphenylmethoxy-1-[3-(2-methanesulfonylaminophenoxy)propyl]-piperidine obtained in Example 1 (c) and then 0.234 g of fumaric acid. The mixture was dried under reduced pressure to form a solid. The residue was recrystallized from isopropyl alcohol to give 0.98 g of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05190959 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-97ec9733be744922a5742f867efb16d3 |
| Source note | uspto-grants-1993_03 |