HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19776700, compound → HCID 19776701, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19776700 | HCID 19776700 | — |
| Solvent | Sodium Carbonate | HCID 10340 | — |
| Product | HCID 19776701 | HCID 19776701 | 89.7% |
Reaction Steps
In 20 ml of 5% aqueous sodium carbonate solution was suspended 1.0 g of the hydrochloride obtained in the above. The resultant solution was extracted with ethyl acetate and the organic layer was washed with water. The solvent was removed under reduced pressure to give 0.83 g of oily 4-(phenyl-2-thienylmethoxy)-1-[3-(2-nitrophenoxy)propyl]piperidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05190959 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-9dbb9f56fb9241d1ae87ec2b951c7ee4 |
| Source note | uspto-grants-1993_03 |