Pyridine → HCID 67884295, compound

Participants

Reaction Steps

To a solution of 16.2 g (0.05 mole) of N-[2-(2-phenyl-2-ethylacetoxy)ethyl]-N'-(3,4,5-trimethoxybenzoyl)piperazine and 4.75 g (0.06 mole) of pyridine in 50 ml of anhydrous chloroform 10.0 g (0.055 mole) of 2-phenyl-2-ethylacetyl chloride were added dropwise. The reaction mixture, treated as described in Example 1 yield the title product. M.p. 207° C. (ethanol).

Provenance & Evidence