HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19777265, compound → 2-(Ethoxymethyl)morpholine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19777265 | HCID 19777265 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(Ethoxymethyl)morpholine | HCID 19777259 | 70.9% |
Reaction Steps
4-Benzyl-2-ethoxymethylmorpholine (1.6 g) and 10% palladium-carbon (200 mg) are added to ethanol (30 ml), and the mixture is stirred under hydrogen pressure of 5 kg/cm2 for 24 hours. Palladium-carbon is filtered off, and the solvent is distilled off under reduced pressure to give the title compound (0.7 g) as colorless liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05191079 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-05839dc1ea714cb08a852c0cb9bc949f |
| Source note | uspto-grants-1993_03 |