Acetic Anhydride → HCID 13349555, compound

HRID 1613003Notes

Reaction equation

HRID 1613003 reaction equation
[CH3:1][C:2](O)([CH2:7][CH2:8][CH:9]=[CH2:10])[CH2:3][C:4](O)=[O:5].C(OC(=O)C)(=O)C.C([O-])(=O)C.[K+]>>[CH3:10][C:9]1[CH:3]2[CH:2]([CH2:7][CH:8]=1)[CH2:1][C:4]2=[O:5]

Participants

4

Reactant 3

HCID 7918Acetic AnhydrideHCID 517044Potassium AcetateHCID 109865133-Hydroxy-3-methylhept-6-enoic acid

Product 1

HCID 13349555HCID 13349555, compound

Procedure

2.07 g (0.013 moles) of 3-methyl-3-hydroxy-hept-6-enoic acid, 15 ml of acetic anhydride and 3 g of potassium acetate are charged into a 50 ml flask equipped with a reflux condenser fitted with a CaCl2 tube.

Workup

  1. customequipped with a reflux condenser
  2. customfitted with a CaCl2 tube

Sources & evidence

ORD record
ord-f8e44d79cc994132aaae3a68e6c49825
Source dataset
uspto-grants-1993_03
Patent number
US05191125

Reaction notes

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