HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Diphenylmethoxymethyl-1-(4-methoxyphenethylamino)cyclohexane → 1-Diphenylmethoxymethyl-1-[N-(4-methoxyphenethyl)-N-methylamino]-cyclohexane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Diphenylmethoxymethyl-1-(4-methoxyphenethylamino)cyclohexane | HCID 19775300 | — |
| Reactant | Sodium cyanoborohydride formaldehyde | HCID 131717802 | — |
| Product | 1-Diphenylmethoxymethyl-1-[N-(4-methoxyphenethyl)-N-methylamino]-cyclohexane | HCID 19775315 | — |
Reaction Steps
The title compound was prepared as described in Example 5, Method A, using 1-diphenylmethoxymethyl-1-(4-methoxyphenethylamino)cyclohexane (see Example 4) and sodium cyanoborohydride/formaldehyde. The title compound was obtained as a colourless oil (0.58 g, 66%), which was characterised from its 1H-n.m.r. spectrum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05192765 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-dc8d9ab8baa4414e8a6d89cebc519ea9 |
| Source note | uspto-grants-1993_03 |