HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 24838526, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Glycine, N-(aminothioxomethyl)- | HCID 3040094 | — |
| Reactant | HCID 19775550 | HCID 19775550 | — |
| Product | HCID 24838526 | HCID 24838526 | — |
Reaction Steps
7.6 g of 3-chloro-4-(4-nitrophenyl)butan-2-one and 4.5 g of N-carboxymethylthiourea (NH2CSNHCH2COOH) are dissolved in 100 ml of ethanol and refluxed for 12 hours. The reaction medium is concentrated and the residue is recrystallized from isopropanol to give 9.5 g of ethyl (4-methyl-5-(4-nitrobenzyl)thiazol-2-yl)aminoacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05192781 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-bf0eaaaf71164490ac7f6f43c2af4ad0 |
| Source note | uspto-grants-1993_03 |