HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 14985850, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Chloro-N,N-dimethylformiminium chloride | HCID 77311 | — |
| Reactant | HCID 14985849 | HCID 14985849 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 14985850 | HCID 14985850 | — |
Reaction Steps
4.9 g of N-((1-(2-acetylaminoethyl)-5-methyl-1H-pyrrol-2-yl)methyl)acetamide in 70 ml of 1,2-dichloroethane are added dropwise to 3.0 g (21 mmol) of chloromethylenedimethylammonium chloride in 30 ml of 1,2-dichloroethane at 10° C. The mixture is subsequently stirred for 90 min, hydrolysed using potassium carbonate solution and worked up as described in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05192795 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-ca1d7539e3f84f108a9749674f0f0858 |
| Source note | uspto-grants-1993_03 |