HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → N-[5-(6-Methoxynaphthalen-1-yl)-1,3-dioxan-2-yl]-methylacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | N-(2,2-Dimethoxyethyl)acetamide | HCID 15289457 | — |
| Reactant | 2-(6-Methoxynaphthalen-1-YL)propane-1,3-diol | HCID 15345801 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | N-[5-(6-Methoxynaphthalen-1-yl)-1,3-dioxan-2-yl]-methylacetamide | HCID 67859839 | — |
Reaction Steps
2.3 g (10 mmol) of 2-(6-methoxynaphthalen-1-yl)propane-1,3-diol, 0.45 g of paratoluenesulphonic acid and 1.6 g (11 mmol) of N-(2,2-dimethoxyethyl)acetamide are introduced into a flask containing 200 ml of benzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05192797 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-8c5558adc9ab4f3c8141be9bf3171969 |
| Source note | uspto-grants-1993_03 |