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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1613455Generated: November 1, 2026

Diethyl Ether → HCID 86745598, compound

https://huagongshe.com/reaction/1613455

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl EtherHCID 3283—
Reactant2-Naphthalenesulfonic acidHCID 8420—
ReactantHCID 54086927HCID 54086927—
ProductHCID 86745598HCID 86745598—

Reaction Steps

A 0.75 g portion of the cyclopropylaminoindole compound was dissolved in 75 ml Et2O and stirred while a solution of 0.69 g of 2-naphthalene sulfonic acid in 50 ml Et2O was added slowly. A white precipitate formed which was filtered under N2, washed with 2×50 ml Et2O and dried to afford 1.04 g of 4-methyl-1,2,3,4-tetrahydrocyclopent[b]indol-3-cyclopropylamine 2-naphthalene sulfonate.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05192789
Source datasetuspto-grants-1993_03
ORD IDord-56f26e8d15454450b38b2a149eca496c
Source noteuspto-grants-1993_03