HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 10445031, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 13069073 | HCID 13069073 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 10445031 | HCID 10445031 | 96% |
Reaction Steps
4-(benzocyclobutan-1-yl)-butyl mesylate was prepared, in a yield of 96%, by treating 4-(benzocyclobutan-1-yl)butanol (oil) with CH3SO2Cl in the presence of triethylamine in methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05194437 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-73d2109ced88471cb13be814be0a9eeb |
| Source note | uspto-grants-1993_03 |