Triethylamine → HCID 10445031, compound

HRID 1613568Notes

Reaction equation

HRID 1613568 reaction equation
[CH:1]1([CH2:9][CH2:10][CH2:11][CH2:12][OH:13])[C:4]2[CH:5]=[CH:6][CH:7]=[CH:8][C:3]=2[CH2:2]1.[CH3:14][S:15](Cl)(=[O:17])=[O:16].C(N(CC)CC)C>C(Cl)Cl>[S:15]([O:13][CH2:12][CH2:11][CH2:10][CH2:9][CH:1]1[C:4]2[CH:5]=[CH:6][CH:7]=[CH:8][C:3]=2[CH2:2]1)(=[O:17])(=[O:16])[CH3:14]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 31297Methanesulfonyl chlorideHCID 13069073HCID 13069073, compound

Product 1

HCID 10445031HCID 10445031, compoundYield 96%

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

4-(benzocyclobutan-1-yl)-butyl mesylate was prepared, in a yield of 96%, by treating 4-(benzocyclobutan-1-yl)butanol (oil) with CH3SO2Cl in the presence of triethylamine in methylene chloride.

Sources & evidence

ORD record
ord-73d2109ced88471cb13be814be0a9eeb
Source dataset
uspto-grants-1993_03
Patent number
US05194437

Reaction notes

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