HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Indanone → 1H-Indene-3-acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Indanone | HCID 6735 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Ethyl (2,3-dihydro-1H-inden-1-ylidene)acetate | HCID 53401861 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 1H-Indene-3-acetic acid | HCID 3014022 | 90% |
Reaction Steps
2-(ind-1-en-1-yl)-acetic acid was prepared according to the method of H. Ahmed and N. Campbell J.C.S. (1960), 4115-4120, in a yield of 90%, from ethyl 2-(indan-1-ylidene)-acetate, which was itself prepared in a yield of 48% from indan-1-one and (C6H5)3P=CH--COOC2H5 in toluene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05194437 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-9c587f65558c4875a69a3f7ec0361f3c |
| Source note | uspto-grants-1993_03 |