Hydrochloric Acid → HCID 14835957, compound

HRID 1613587Notes

Reaction equation

HRID 1613587 reaction equation
O[N:2]([CH2:14][CH2:15][CH3:16])[CH:3]1[CH2:12][C:11]2[N:10]=[CH:9][C:8]([CH3:13])=[CH:7][C:6]=2[CH2:5][CH2:4]1.Cl>[Cl-].[Cl-].[Cl-].[Ti+3].CO>[CH3:13][C:8]1[CH:9]=[N:10][C:11]2[CH2:12][CH:3]([NH:2][CH2:14][CH2:15][CH3:16])[CH2:4][CH2:5][C:6]=2[CH:7]=1

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 14835956HCID 14835956, compound

Product 1

HCID 14835957HCID 14835957, compound

Reagents, catalysts & solvents 2

HCID 10313229titanium(III) trichlorideCatalystHCID 887MethanolSolvent

Procedure

This compound was prepared from the product of Step 3 (4.45 g, 20 mmol), titanium trichloride, 20 wt. % solution in 20 wt. % hydrochloric acid (23 ml, 30 mmol), and methanol (50 ml) using the procedure described in Example 11. The crude amine (4.0 g) was converted directly into the product of Step 5.

Sources & evidence

ORD record
ord-9811d613120041daa88b4631df403b97
Source dataset
uspto-grants-1993_03
Patent number
US05194439

Reaction notes

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