HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → 4-Chloro-5,6-dihydroquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 4-Chloro-5,6,7,8-tetrahydro-8-(phenylseleno)quinoline | HCID 14835961 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 4-Chloro-5,6-dihydroquinoline | HCID 14835962 | 93.8% |
Reaction Steps
This compound was prepared from the product of Step 3 (9 g, 28 mmol), 86% 3-chloroperoxybenzoic acid (5.8 g, 29 mmol), and dichloromethane (150 ml) using the procedure outlined in Example 25. Step 2. Distillation gave the product (4.35 g) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05194439 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-d9a66b36368f49dea5235a76e3858063 |
| Source note | uspto-grants-1993_03 |