反应详情

This compound was prepared from the product of Step 3 (9 g, 28 mmol), 86% 3-chloroperoxybenzoic acid (5.8 g, 29 mmol), and dichloromethane (150 ml) using the procedure outlined in Example 25. Step 2. Distillation gave the product (4.35 g) as an oil.

1. distillationDistillation