HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → N-(4-Methylvaleryloxyethyl)-N,N-dimethylbenzylammonium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | 2-(N,N-Dimethylamino)ethyl 4-methylvalerate | HCID 19774313 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N-(4-Methylvaleryloxyethyl)-N,N-dimethylbenzylammonium chloride | HCID 86745753 | — |
Reaction Steps
A solution of 46.83 g (0.25 mol) of 2-(N,N-dimethylamino)ethyl 4-methylvalerate (prepared as described in Example 1) and 31.65 g (0.25 mol) of benzyl chloride in 250 ml of acetonitrile was heated at reflux for 1.25 hours. The reaction mixture was then concentrated to a viscous oil and used in the ion exchange step with no further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05194472 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-411730d338e9419c976b1fbd34abada0 |
| Source note | uspto-grants-1993_03 |