HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexachloroethane → HCID 14949194, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexachloroethane | HCID 6214 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 4-Fluoro-N-(trimethylsilyl)benzene-1-sulfonamide | HCID 14949189 | — |
| Product | HCID 14949194 | HCID 14949194 | — |
Reaction Steps
The reactants used in the general procedure were hexachloroethane (0.0953 mol, 23.02 g), triphenylphosphine (0.0963 mol, 25.51 g), triethylamine (0.0991 mol, 12.5 ml), and a mixture of N-mono- and N,N-bis(trimethylsilyl sulfonamides (3c) and (5c) containing about 89.5% monosilylsulfonamide (3c) (0.0881 mol, 21.76 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05194557 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-173244f6f8ad4ca19d588b462e3b7972 |
| Source note | uspto-grants-1993_03 |