HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexachloroethane → HCID 14949190, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexachloroethane | HCID 6214 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | N-(Trimethylsilyl)ethanesulfonamide | HCID 14949186 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 14949190 | HCID 14949190 | — |
Reaction Steps
Hexachloroethane (0.1110 mol, 26.81 g), triphenylphosphine (0.1121 mol, 29.70 g), triethylamine (0.1110 mol, 15.7 mL), monosilylsulfonamide (3f) (0.1110 mol, 20.1 g). 1H NMR signals (90 MHz, CHCl3): 0.00 (s, 9H), 1.27 (t, 3H), 3.23 (q, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05194557 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-c5232614a8594e2da876361adb01bf01 |
| Source note | uspto-grants-1993_03 |