HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 14949203, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 14949194 | HCID 14949194 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 14949203 | HCID 14949203 | 15% |
Reaction Steps
The reactants used in the general procedure were sulfonimidoyl chloride (7c), triethylamine (0.0936 mol, 13.3 ml), phenol (0.0934 mol, 8.79 g). Boiling range of product: 125°-131° C./0.25 mm. Yield: 15%. 1H NMR signals (90 MHz, CH3CN): 0.24 (s, 9H), 6.83-7.57 (m, 7H), and 7.83-8.1 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05194557 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-4e07a3e6d6c349e7ada6c1a2b8c9d673 |
| Source note | uspto-grants-1993_03 |