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HRID 1614251作成日：2026年10月25日

Allylamine hydrochloride → 5-Acetylamino-2-allylamino-tetraline-hydrochloride

https://huagongshe.com/reaction/1614251

反応式

関与物質

役割名称HCID仕込み量
反応物Allylamine hydrochlorideHCID 82291—
反応物5-Acetylamino-2-tetraloneHCID 14836456—
生成物5-Acetylamino-2-allylamino-tetraline-hydrochlorideHCID 19773280—

反応手順

Starting from 3.04 g (0.015 mol) of 5-acetylamino-2-tetralone and 4.2 g (0.045 mol) of allylaminehydrochloride the title compound is obtained analogously to Example 4.1.11 in a yield of 3.30 g (78.4% of theory) and with a melting point of 263° C. which does not change after recrystallisation from methanol/water/ether.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05196454
出典データセットuspto-grants-1993_03
ORD IDord-bcbcebbd273e4d2ba19cbe79258b957b
出典メモuspto-grants-1993_03