HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dopamine → HCID 19773395, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dopamine | HCID 681 | — |
| Reactant | 2-(Furan-2-yl)ethan-1-amine hydrochloride | HCID 13045548 | — |
| Reactant | 5-Acetylamino-2-tetralone | HCID 14836456 | — |
| Product | HCID 19773395 | HCID 19773395 | — |
Reaction Steps
Starting from 0.61 g (0.0031 mol) of 5-acetylamino-2-tetralone and 0.9 g (0.006 mol) of 2 (2-furyl)ethylamine-hydrochloride the title compound is obtained analogously to Example 4.1.11 in a yield of 0.8 g (77.1% of theory) and with a melting point of 256° C., which increases to 257° C. after recrystallisation from methanol/ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05196454 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-4792ae63847248e18762df49d636f09b |
| Source note | uspto-grants-1993_03 |