HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine, hydrochloride → HCID 19773352, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine, hydrochloride | HCID 10473 | — |
| Reactant | 5-Acetylamino-2-tetralone | HCID 14836456 | — |
| Product | HCID 19773352 | HCID 19773352 | — |
Reaction Steps
Starting from 2.03 g (0.01 mol) of 5-acetylamino-2-tetralone and 2.45 g (0.03 mol) of dimethylaminehydrochloride the title compound is obtained analogously to Example 4.1.11 in a yield of 1.35 g (50.2% of theory) and with a melting point of 199° C. which does not change after recrystallisation from methanol/ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05196454 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-1cefde5815b94050a8cdb7d754e65348 |
| Source note | uspto-grants-1993_03 |