HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 14822258, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | N-[4-(4-aminophenyl)butanoyl]thiazolidine | HCID 14822257 | — |
| Product | HCID 14822258 | HCID 14822258 | 98% |
Reaction Steps
To 5 ml of alcoholic hydrogen chloride 1 mmol of N-[4-(4-aminophenyl)butanoyl]thiazolidine was added and dissolved under heating. The mixture was stirred at room temperature for 2 hours. After the reaction, the solvent was evaporated under reduced pressure. To the residue was added anhydrous ether and precipitates thus produced were collected by filtration to obtain 0.28 g of colorless crystals of N-[4-(4-aminophenyl)butanoyl]thiazolidine hydrochloride (yield: 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05198450 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-dd4eea7a48f64c49a0fdc4e86b926e08 |
| Source note | uspto-grants-1993_03 |