HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 19772096, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | HCID 19772068 | HCID 19772068 | — |
| Product | HCID 19772096 | HCID 19772096 | — |
Reaction Steps
1-(3-Chloropropyl)-N,α-bis(4-fluorophenyl)-4-piperidinemethanamine and excess aniline are heated together until the reaction is complete. Excess aniline is distilled off and the residual material partitioned between dilute aqueous sodium hydroxide and methylene chloride. The methylene chloride solution is dried and concentrated to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05198449 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-bc677eb7c087400fa846399434db0276 |
| Source note | uspto-grants-1993_03 |