HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → 4-[(Trifluoroethenyl)oxy]phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | HCID 19763912 | HCID 19763912 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 4-[(Trifluoroethenyl)oxy]phenol | HCID 19772420 | — |
Reaction Steps
A sample of 4-trifluoroethenyloxyanisole prepared as in Example 2 is treated with two equivalents of trimethylchlorosilane and sodium iodide in refluxing acetonitrile to give 4-trifluoroethenyloxyphenol. The product is extracted with ether, washed with sodium thiosulfate solution to remove iodine, and then concentrated by rotary evaporation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05198513 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-e3dfbbf41a5e4cd1b4a5bb76646dad24 |
| Source note | uspto-grants-1993_03 |