HRID1614697

反应详情

EQUATION

反应方程式

HRID 1614697 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

D (-)-3,3-Diphenylalanine hydrochloride (0.5 g) is dissolved in 15 mL of water and the pH of the solution is adjusted with dilute ammonium hydroxide solution to pH 7. The precipitate is collected by filtration, washed with water, boiled with water for a short time, cooled to room temperature, and collected to afford 0.2 g of the title compound; mp 218°-220° C. (dec.).

WORKUP

后处理

  1. filtrationThe precipitate is collected by filtration
  2. washwashed with water
  3. customcollected