Salicylic Acid → HCID 178525430, compound

HRID 1614716Notes

Reaction equation

[C:1]([OH:12])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]([OH:10])=[O:9].[C:13]([OH:22])(=[O:21])[C:14]1[C:15](=[CH:17][CH:18]=[CH:19][CH:20]=1)[OH:16].C(OC(=O)C)(=O)C>>[C:13]([O-:22])(=[O:21])[C:14]1[C:15](=[CH:17][CH:18]=[CH:19][CH:20]=1)[OH:16].[C:1]([O-:12])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]([O-:10])=[O:9]

Participants

Reactant 3

HCID 338Salicylic Acid

HCID 7918Acetic Anhydride

HCID 10457Suberic acid

Product 1

HCID 178525430HCID 178525430, compound

Procedure

The procedure described in Example 1, above, was used with suberic acid (315 g, 1.8 mol), salicylic acid (250 g, 1.8 mol) and 725 mL acetic anhydride. The reaction mixture formed a clear solution and then a clear melt and the final product was a light colored, transparent, slightly fluid glass which weighed 489 g. NMR spectra indicated very little acetate and no starting materials were present.

Workup

customThe reaction mixture formed a clear solution

Sources & evidence

ORD record: ord-31effe471ddb4730abe28edd4d2230e1
Source dataset: uspto-grants-1993_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05198572

Reaction notes

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