Salicylic Acid → HCID 178525425, compound

HRID 1614717Notes

Reaction equation

HRID 1614717 reaction equation
[C:1]([OH:14])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]([OH:12])=[O:11].[C:15]([OH:24])(=[O:23])[C:16]1[C:17](=[CH:19][CH:20]=[CH:21][CH:22]=1)[OH:18]>C(OC(=O)C)(=O)C>[C:15]([O-:24])(=[O:23])[C:16]1[C:17](=[CH:19][CH:20]=[CH:21][CH:22]=1)[OH:18].[C:1]([O-:14])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]([O-:12])=[O:11]

Participants

4

Reactant 2

HCID 338Salicylic AcidHCID 5192Sebacic Acid

Product 1

HCID 178525425HCID 178525425, compound

Reagents, catalysts & solvents 1

HCID 7918Acetic AnhydrideSolvent

Procedure

The procedure described in Example 1, above was used with sebacic acid (50 g, 0.5 mol), salicylic acid (69 g, 0.5 mol) and 200 mL acetic anhydride. The reaction mixture formed a clear solution and then a clear melt and the final product was a dark colored, transparent, slightly fluid glass which weighed 127 g. NMR spectra indicated very little acetate and no starting materials were present.

Workup

  1. customThe reaction mixture formed a clear solution

Sources & evidence

ORD record
ord-e3fdd851903842e3ae37c1f1c090d7c9
Source dataset
uspto-grants-1993_03
Patent number
US05198572

Reaction notes

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