反应详情

To a solution of 1-(2-methylphenyl)-1-phenyl-1-propene (9.0 g, 43 mmol) in carbon tetrachloride (40 ml), N-bromosuccinimide (7.7 g, 43 mmol) and benzoylperoxide (0.1 g) were added. The reaction mixture was heated at reflux temperature for 18 h. The cooled reaction mixture was filtered through silica gel and the solvent evaporated in vacuo to give 9.3 g (76%) of 3-bromo-1-(2-methylphenyl)-1-phenyl-1-propene.

1. temperatureThe reaction mixture was heated
2. temperatureat reflux temperature for 18 h
3. customThe cooled reaction mixture
4. filtrationwas filtered through silica gel
5. customthe solvent evaporated in vacuo