HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 54536217, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 1-(2-Methylphenyl)-1-phenyl-1-propene | HCID 54442405 | — |
| Catalyst | Benzoyl Peroxide | HCID 7187 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 54536217 | HCID 54536217 | 76% |
Reaction Steps
To a solution of 1-(2-methylphenyl)-1-phenyl-1-propene (9.0 g, 43 mmol) in carbon tetrachloride (40 ml), N-bromosuccinimide (7.7 g, 43 mmol) and benzoylperoxide (0.1 g) were added. The reaction mixture was heated at reflux temperature for 18 h. The cooled reaction mixture was filtered through silica gel and the solvent evaporated in vacuo to give 9.3 g (76%) of 3-bromo-1-(2-methylphenyl)-1-phenyl-1-propene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05198451 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-1a21857d5c754670af119f208e6cb737 |
| Source note | uspto-grants-1993_03 |